Works Published in 2005
Displaying works 61 - 80 of 219 in total
Sorted by most recent date added to the index first, which may not be the same as publication date order.
2005 journal article
Low power upconversion using MLCT sensitizers
Chemical Communications, (30), 3776.
Contributors: R. Islangulov*, D. Kozlov* & F. Castellano*
TL;DR:
Selective low energy excitation of the metal-to-ligand charge transfer (MLCT) transition in [Ru(dmb)(3)](2+)(dmb = 4,4'-dimethyl-2,2'-bipyridine) in the presence of anthracene or 9,10-diphenylanthracene yields easily visualized upconverted singlet fluorescence resulting from triplet-triplet annihilation at low excitation power.
(via Semantic Scholar)
UN Sustainable Development Goal Categories
7. Affordable and Clean Energy
(OpenAlex)
Sources: Crossref, ORCID, NC State University Libraries
Added: August 28, 2020
2005 journal article
Green Photoluminescence from Platinum(II) Complexes Bearing Silylacetylide Ligands
Inorganic Chemistry, 44(3), 471–473.
Contributors: F. Hua*, S. Kinayyigit*, J. Cable* & F. Castellano*
scholarworks.bgsu.edu (repository)
UN Sustainable Development Goal Categories
7. Affordable and Clean Energy
(OpenAlex)
Sources: Crossref, ORCID, NC State University Libraries
Added: August 28, 2020
2005 journal article
Synthesis of Homoallylic Amines by Hydrozirconation−Imine Addition of Allenes
Organic Letters, 7(16), 3537–3540.
TL;DR:
Hydrozirconation of allenes followed by in situ transmetalation to dialkylzinc leads to the formation of an allylic zinc species that, upon addition of aldimines to the reaction mixture, provides homoallylic amines in 64-85% yield.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Silver(I)-Catalyzed Addition of Zirconocenes to Glycal Epoxides. A New Synthesis of α-C-Glycosides
Organic Letters, 7(3), 483–485.
MeSH headings : Catalysis; Epoxy Compounds / chemical synthesis; Glycosides / chemical synthesis; Indicators and Reagents; Molecular Conformation; Organometallic Compounds / chemistry; Silver / chemistry; Stereoisomerism; Zirconium / chemistry
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Mechanism for Reduction Catalysis by Metal Oxo: Hydrosilation of Organic Carbonyl Groups Catalyzed by a Rhenium(V) Oxo Complex
Journal of the American Chemical Society, 127(44), 15374–15375.
TL;DR:
The rhenium oxo complex catalyzes the hydrosilation of aldehydes and ketones under ambient temperature and atmosphere and a viable mechanism that is consistent with experimental findings, rate measurements, and kinetic isotope effects is proposed.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Mapping Sites of Protein Phosphorylation by Mass Spectrometry Utilizing a Chemical-Enzymatic Approach: Characterization of Products from α-S1Casein Phosphopeptides
Journal of Proteome Research, 4(2), 424–434.
author keywords: chemical-enzymatic; phosphorylation; 2-aminoethanethiol; isotope dilution mass spectrometry; phosphoproteins; phosphopeptides; quantification
MeSH headings : Amino Acid Sequence; Animals; Caseins / metabolism; Cattle; Molecular Sequence Data; Peptide Fragments / metabolism; Phosphopeptides / metabolism; Phosphorylation; Spectrometry, Mass, Electrospray Ionization / methods
TL;DR:
ESI-TOF mass spectrometry was used to characterize products from the chemical-enzymatic cleavage of specific phosphorylation sites in bovine alpha-S1 casein and synthetic phosphopeptides containing substitutions at a single phosphorylated site.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Protein expression profiling of CLL B cells using replicate off-line strong cation exchange chromatography and LC–MS/MS
Journal of Chromatography B, 819(1), 33–39.
author keywords: CLL; 2D-LC-MS/MS; B cell; expression profiling; off-line SCX; reproducibility
MeSH headings : Antigens, CD / isolation & purification; B-Lymphocytes / metabolism; Blood Proteins / isolation & purification; Cell Fractionation; Cell Membrane / chemistry; Chromatography, Ion Exchange / methods; Chromatography, Liquid / methods; Gene Expression Profiling / methods; Humans; Leukemia, Lymphocytic, Chronic, B-Cell / metabolism; Mass Spectrometry / methods; Neoplasm Proteins / blood
TL;DR:
Examination of crude membranes from B cells derived from a patient with chronic lymphocytic leukemia to examine the protein expression profile of CLL B cells shows an overlap of 64% between proteins identified in replicate runs was achieved for this system.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Déjà Vu All Over Again: Skin Cap Still Contains a High-Potency Glucocorticosteroid
Archives of Dermatology, 141(6).
MeSH headings : Administration, Topical; Adrenal Cortex Hormones / adverse effects; Adrenal Cortex Hormones / chemistry; Adrenal Cortex Hormones / therapeutic use; Chemistry, Pharmaceutical; Dermatologic Agents / adverse effects; Dermatologic Agents / pharmacology; Dermatologic Agents / therapeutic use; Female; Humans; Male; Materials Testing; Psoriasis / diagnosis; Psoriasis / drug therapy; Risk Assessment; Sensitivity and Specificity
Sources: Crossref, NC State University Libraries
Added: August 28, 2020
2005 journal article
Flow Control through Polymer-Grafted Smart Nanofluidic Channels: Molecular Dynamics Simulations
Nano Letters, 5(12), 2509–2514.
MeSH headings : Computer Simulation; Computer-Aided Design; Equipment Design; Equipment Failure Analysis; Microfluidics / instrumentation; Microfluidics / methods; Models, Chemical; Models, Molecular; Motion; Nanotechnology / instrumentation; Nanotechnology / methods; Polymers / chemistry; Solvents / chemistry
TL;DR:
Results of molecular dynamics simulations demonstrate flow gating through a polymer-grafted nanopore as a function of effective solvent quality and establish a critical starting point in nanofluidics from which continuum modeling can be developed to design this emerging class of smart nanoporous materials with tailor-made properties.
(via Semantic Scholar)
Source: Crossref
Added: August 28, 2020
2005 journal article
Synthesis and Reactivity of Molybdenum(IV) Complexes with Alkyl and Aryl Isocyanides
Organometallics, 24(26), 6310–6318.
UN Sustainable Development Goal Categories
6. Clean Water and Sanitation
(OpenAlex)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Hydrogen Production from Hydrolytic Oxidation of Organosilanes Using a Cationic Oxorhenium Catalyst
Journal of the American Chemical Society, 127(34), 11938–11939.
TL;DR:
The novel application of a transition metal oxo complex, a cationic oxorhenium(V) oxazoline, in the production of molecular hydrogen (H2) from the catalytic hydrolytic oxidation of organosilanes is described.
(via Semantic Scholar)
UN Sustainable Development Goal Categories
6. Clean Water and Sanitation
(OpenAlex)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Quantitative mass spectral evidence for the absence of circulating brain natriuretic peptide (BNP-32) in severe human heart failure
Proceedings of the National Academy of Sciences, 102(48), 17442–17447.
author keywords: biomarkers; electrospray ionization; Fourier transform-ion cyclotron resonance MS; immunoaffinity purification; targeted proteomics
MeSH headings : Chromatography, Liquid; Female; Heart Failure / metabolism; Humans; Isotope Labeling; Male; Mass Spectrometry; Natriuretic Peptide, Brain / blood; Natriuretic Peptide, Brain / isolation & purification
TL;DR:
An immunoaffinity purification assay is developed and used to isolate endogenous BNP-32 from New York Heart Association class IV patient plasma for subsequent analysis by nano-liquid chromatography (LC) electrospray ionization Fourier transform ion cyclotron resonance (FT-ICR) MS.
(via Semantic Scholar)
UN Sustainable Development Goal Categories
3. Good Health and Well-being
(OpenAlex)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Evaluation of Protein Depletion Methods for the Analysis of Total-, Phospho- and Glycoproteins in Lumbar Cerebrospinal Fluid
Journal of Proteome Research, 4(3), 837–845.
author keywords: cerebrospinal fluid; human; two-dimensional gel electrophoresis; mass spectrometry; glycoprotein; phosphoprotein; protein depletion; low-abundance protein
MeSH headings : Adult; Aged; Cerebrospinal Fluid Proteins / analysis; Cerebrospinal Fluid Proteins / classification; Cerebrospinal Fluid Proteins / isolation & purification; Chromatography, Affinity; Electrophoresis, Gel, Two-Dimensional; Female; Fluorescent Dyes; Glycoproteins / cerebrospinal fluid; Glycoproteins / isolation & purification; Humans; Immunoglobulins; Male; Mass Spectrometry; Methods; Microspheres; Middle Aged; Phosphoproteins / cerebrospinal fluid; Phosphoproteins / isolation & purification
TL;DR:
Phospho- and glycoprotein specific fluorescent stains and mass spectrometry were used to map proteins from CSF on two-dimensional gel electropherograms after immunoaffinity based protein removal, and fifty proteins were identified from 66 spots, and 12 proteins have not been annotated in previously published 2D gels.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Coordination-Driven Self-Assemblies with a Carborane Backbone
Journal of the American Chemical Society, 127(34), 12131–12139.
MeSH headings : Boranes / chemistry; Crystallography, X-Ray; Isotope Labeling; Magnetic Resonance Spectroscopy; Molecular Structure; Pyridines / chemistry; Spectrometry, Mass, Electrospray Ionization
TL;DR:
Isotopically resolved mass spectrometry data confirm the existence of the rectangle, triangle, and hexagon, and NMR data are consistent with the formation of all five assemblies.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Gentle Protein Ionization Assisted by High-Velocity Gas Flow
Analytical Chemistry, 77(19), 6174–6183.
MeSH headings : Cytochromes c / chemistry; Hydrogen-Ion Concentration; Ions / chemistry; Myoglobin / chemistry; Proteins / chemistry; Spectrometry, Mass, Electrospray Ionization / instrumentation; Spectrometry, Mass, Electrospray Ionization / methods; Ubiquitin / chemistry
TL;DR:
Evidence is provided for the importance of the conditions used in the desolvation process for the preservation of the protein conformation and suggest that the conditions achieved when using high-velocity gas flows to assist droplet evaporation and ion Desolvation are much gentler than those in conventional ESI experiments.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Statistical Evaluation of Internal and External Mass Calibration Laws Utilized in Fourier Transform Ion Cyclotron Resonance Mass Spectrometry
Analytical Chemistry, 77(8), 2406–2414.
MeSH headings : Calibration; Cyclotrons; Data Interpretation, Statistical; Fourier Analysis; Polymers / analysis; Polymers / chemistry; Propylene Glycols / analysis; Propylene Glycols / chemistry; Quaternary Ammonium Compounds / chemistry; Reproducibility of Results; Sensitivity and Specificity; Spectrometry, Mass, Electrospray Ionization / methods
TL;DR:
The statistical evaluation of two common and three new calibration laws utilized in Fourier transform ion cyclotron resonance mass spectrometry are presented and the number of calibrant ions as well as their required m/z range is investigated in order to successfully achieve high MMA.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Derivatives of pentamidine designed to target the Leishmania lipophosphoglycan
Tetrahedron Letters, 46(4), 695–698.
author keywords: boronate drug targeting; pentamidine; Leishmania
TL;DR:
Pentamidine has been modified with boronic acids so that it might bind more selectively to the phosphodisaccharide repeating unit of the LPG, which could serve to target the drug to the protozoan surface and increase its efficacy in vivo.
(via Semantic Scholar)
UN Sustainable Development Goal Categories
3. Good Health and Well-being
(OpenAlex)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Leveling response factors in the electrospray ionization process using a heated capillary interface
Journal of the American Society for Mass Spectrometry, 16(5), 772–778.
MeSH headings : Capillary Action; DNA / analysis; DNA / chemistry; Equipment Design; Equipment Failure Analysis; Hot Temperature; Humans; Specimen Handling / instrumentation; Specimen Handling / methods; Spectrometry, Mass, Electrospray Ionization / instrumentation; Spectrometry, Mass, Electrospray Ionization / methods
TL;DR:
The implementation of a heated electrospray source was used to denature amplicons containing 7-deaza purines, which can be used to facilitate sequencing by mass spectrometry.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Normalization of relative peptide ratios derived from in-gel digests: applications to protein variant analysis at the peptide level
Rapid Communications in Mass Spectrometry, 19(19), 2871–2877.
MeSH headings : Algorithms; Chromatography, High Pressure Liquid / methods; Gas Chromatography-Mass Spectrometry / methods; Gas Chromatography-Mass Spectrometry / standards; Humans; Osmotic Fragility; Peptide Mapping / methods; Peptide Mapping / standards; Reference Values; Reproducibility of Results; Sensitivity and Specificity; Spectrin / analysis; Spectrin / chemistry; Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / methods
TL;DR:
A strategy was developed to normalize for sample variability due to ionization efficiency, solvent effects, digestion and extraction efficiency by utilizing multiple isotopically labeled internal standards for multiple peptides derived from the same protein.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
2005 journal article
Effect of post-excitation radius on ion abundance, mass measurement accuracy, and isotopic distributions in Fourier transform ion cyclotron resonance mass spectrometry
Rapid Communications in Mass Spectrometry, 19(7), 915–918.
MeSH headings : Bradykinin / analysis; Ions; Isotopes; Reproducibility of Results; Spectroscopy, Fourier Transform Infrared / instrumentation; Spectroscopy, Fourier Transform Infrared / methods; Tritium
TL;DR:
The findings presented herein underscore the importance of determining the optimal post-excitation radius in FT-ICR-MS to achieve high ion abundance (low limits of detection), high MMA, and valid isotopic distributions.
(via Semantic Scholar)
Sources: Crossref, NC State University Libraries
Added: February 24, 2020
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