@article{korobkina_berkutov_golub_huffman_hickman_leung_medlin_morano_rao_teander_et al._2022, title={Growing solid deuterium for UCN production}, volume={24}, ISSN={["1477-2655"]}, DOI={10.3233/JNR-220010}, abstractNote={We have experimentally studied growing a large (about 1 liter) ortho-deuterium crystal in a real UCN source cryostat and recorded the growing process optically using a camera. The best quality was observed when growing the crystal directly from a vapor phase. The crystal was grown at different mass flows of deuterium and annealed at different temperatures. Optimum conditions were found for both, obtaining an optically transparent crystal and cooling it down with minimal damage. We found that the quality, final shape and changes during annealing of the crystal are very much dependent on the temperature profile of the cryostat walls.}, number={2}, journal={JOURNAL OF NEUTRON RESEARCH}, author={Korobkina, Ekaterina and Berkutov, Igor and Golub, Robert and Huffman, Paul and Hickman, Clark and Leung, Kent and Medlin, Graham and Morano, Matthew J. and Rao, Thomas and Teander, Cole and et al.}, year={2022}, pages={179–191} }
 @article{anghel_bailey_bison_blau_broussard_clayton_cude-woods_daum_hawari_hild_et al._2018, title={Solid deuterium surface degradation at ultracold neutron sources}, volume={54}, ISSN={1434-6001 1434-601X}, url={http://dx.doi.org/10.1140/epja/i2018-12594-2}, DOI={10.1140/epja/i2018-12594-2}, abstractNote={Solid deuterium (sD_2) is used as an efficient converter to produce ultracold neutrons (UCN). It is known that the sD_2 must be sufficiently cold, of high purity and mostly in its ortho-state in order to guarantee long lifetimes of UCN in the solid from which they are extracted into vacuum. Also the UCN transparency of the bulk sD_2 material must be high because crystal inhomogeneities limit the mean free path for elastic scattering and reduce the extraction efficiency. Observations at the UCN sources at Paul Scherrer Institute and at Los Alamos National Laboratory consistently show a decrease of the UCN yield with time of operation after initial preparation or later treatment (`conditioning') of the sD_2. We show that, in addition to the quality of the bulk sD_2, the quality of its surface is essential. Our observations and simulations support the view that the surface is deteriorating due to a build-up of D_2 frost-layers under pulsed operation which leads to strong albedo reflections of UCN and subsequent loss. We report results of UCN yield measurements, temperature and pressure behavior of deuterium during source operation and conditioning, and UCN transport simulations. This, together with optical observations of sD_2 frost formation on initially transparent sD_2 in offline studies with pulsed heat input at the North Carolina State University UCN source results in a consistent description of the UCN yield decrease.}, number={9}, journal={The European Physical Journal A}, publisher={Springer Nature}, author={Anghel, A. and Bailey, T. L. and Bison, G. and Blau, B. and Broussard, L. J. and Clayton, S. M. and Cude-Woods, C. and Daum, M. and Hawari, A. and Hild, N. and et al.}, year={2018}, month={Sep} }
 @article{korobkina_medlin_wehring_hawari_huffman_young_beaumont_palmquist_2014, title={Ultracold neutron source at the PULSTAR reactor: Engineering design and cryogenic testing}, volume={767}, ISSN={1872-9576}, DOI={10.1016/j.nima.2014.08.016}, abstractNote={Construction is completed and commissioning is in progress for an ultracold neutron (UCN) source at the PULSTAR reactor on the campus of North Carolina State University. The source utilizes two stages of neutron moderation, one in heavy water at room temperature and the other in solid methane at ~40K, followed by a converter stage, solid deuterium at 5 K, that allows a single down scattering of cold neutrons to provide UCN. The UCN source rolls into the thermal column enclosure of the PULSTAR reactor, where neutrons will be delivered from a bare face of the reactor core by streaming through a graphite-lined assembly. The source infrastructure, i.e., graphite-lined assembly, heavy-water system, gas handling system, and helium liquefier cooling system, has been tested and all systems operate as predicted. The research program being considered for the PULSTAR UCN source includes the physics of UCN production, fundamental particle physics, and material surface studies of nanolayers containing hydrogen. In the present paper we report details of the engineering and cryogenic design of the facility as well as results of critical commissioning tests without neutrons.}, journal={NUCLEAR INSTRUMENTS & METHODS IN PHYSICS RESEARCH SECTION A-ACCELERATORS SPECTROMETERS DETECTORS AND ASSOCIATED EQUIPMENT}, author={Korobkina, E. and Medlin, G. and Wehring, B. and Hawari, A. I. and Huffman, P. R. and Young, A. R. and Beaumont, B. and Palmquist, G.}, year={2014}, month={Dec}, pages={169–175} }