@article{witharamage_christudasjustus_walunj_borkar_gupta_2024, title={Effect of V Content on Corrosion Behavior of Al-V Alloys Produced by Mechanical Alloying and Subsequent Spark Plasma Sintering}, volume={171}, ISSN={["1945-7111"]}, url={https://doi.org/10.1149/1945-7111/ad2d1b}, DOI={10.1149/1945-7111/ad2d1b}, abstractNote={Al-V alloys produced via high-energy ball milling have been reported to show simultaneous improvement of corrosion resistance and mechanical properties compared to traditional Al alloys. In these alloys, V content plays a crucial role in increasing or decreasing the corrosion resistance. Therefore, the effect of V and microstructure on corrosion of high-energy ball milled and subsequently spark plasma sintered Al-xV alloys (x = 2, 5, 10 at%) has been studied. Cyclic potentiodynamic polarization tests and electrochemical impedance spectroscopic analysis revealed the increment of V content up to 5 at% enhanced the corrosion resistance of the alloy. However, highly heterogeneous microstructure in Al-10 at%V resulted in significant localized corrosion over the immersion time. The electrochemical impedance spectroscopy studies over 14 days of immersion revealed underlying corrosion mechanisms.}, number={3}, journal={JOURNAL OF THE ELECTROCHEMICAL SOCIETY}, author={Witharamage, Chathuranga Sandamal and Christudasjustus, J. and Walunj, G. and Borkar, T. and Gupta, R. K.}, year={2024}, month={Mar} } @article{christudasjustus_felde_witharamage_esquivel_darwish_winkler_gupta_2023, title={Age-hardening behavior, corrosion mechanisms, and passive film structure of nanocrystalline Al-V supersaturated solid solution}, volume={135}, ISSN={["1941-1162"]}, url={https://doi.org/10.1016/j.jmst.2022.06.044}, DOI={10.1016/j.jmst.2022.06.044}, abstractNote={The effect of age-hardening on microstructure, hardness, and corrosion of an Al-5at.%V alloy, produced using high-energy ball milling and subsequent cold compaction, has been investigated. The alloy exhibited a grain size below 100 nm and extremely high solid solubility of V in Al (3.1 at.%). The age-hardening was carried out at 150, 200, and 250 °C. The peak-aged condition of 150 °C demonstrated the highest hardness—transpired from grain refinement, precipitation, and solid solution hardening. The corrosion resistance of the Al-5at.%V alloy was studied as a function of aging conditions. The peak-aged condition retained the corrosion resistance while it deteriorated in the over-aged condition. Nonetheless, the corrosion resistance of the ball-milled Al alloys in all the aging conditions was superior to that of pure Al. The passive film structure and origin of corrosion were studied using scanning/transmission electron microscopy (S/TEM). The high corrosion resistance of the alloy was attributed to the V enrichment at the film/metal interface and deposition of V on the cathodic phases, which suppresses the dissolution of Al within the pit and therefore promotes repassivation in the early stages of corrosion.}, journal={JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY}, author={Christudasjustus, J. and Felde, M. R. and Witharamage, C. S. and Esquivel, J. and Darwish, A. . A. . and Winkler, C. and Gupta, R. K.}, year={2023}, month={Feb}, pages={1–12} } @article{christudasjustus_vukkum_gupta_2023, title={Evolution of surface film in AA2024-T3 after a long-term immersion in NaCl solution}, volume={215}, ISSN={["1879-0496"]}, url={http://dx.doi.org/10.1016/j.corsci.2023.111056}, DOI={10.1016/j.corsci.2023.111056}, abstractNote={Surface films of AA2024-T3 after immersion in 0.1 M NaCl for 14 days, 6 months, and 1 year have been investigated using scanning electron microscopy. The corrosion product generated on the surface over the immersion period was comprised of porous outer and compact inner layers. The Cu enrichment at the corrosion product/metal interface and Cu clusters within the surface films have been observed. Exfoliation corrosion was observed, which allows the electrolyte to migrate through exfoliated path and cause rapid corrosion at sub-surface level. Mechanistic aspects of surface film, Cu cluster formation, and corrosion under the surface film have been discussed.}, journal={CORROSION SCIENCE}, publisher={Elsevier BV}, author={Christudasjustus, J. and Vukkum, V. B. and Gupta, R. K.}, year={2023}, month={May} } @article{vukkum_delvecchio_christudasjustus_storck_gupta_2023, title={Intergranular Corrosion of Feedstock Modified-Additively Manufactured Stainless Steel After Sensitization}, volume={79}, ISSN={["1938-159X"]}, url={https://doi.org/10.5006/4245}, DOI={10.5006/4245}, abstractNote={Laser powder bed fusion (LPBF), a metal additive manufacturing technique, was conducted on feedstock-modified 316L stainless steel (316L) powder produced by ball-milling of commercial 316L and 1 wt% additive (cerium oxide—CeO2, lanthanum (III) nitrate hexahydrate—La(NO3)3·6H2O, and chromium nitride—CrN). The feedstock-modified LPBF-316L specimens were sensitized at 675°C for 24 h, and the influence of additives on intergranular corrosion (IGC) was investigated following ASTM G108-94 and A262-14 standards. The LPBF-316L with La(NO3)3·6H2O showed higher IGC resistance. The microstructure of the LPBF specimen was investigated and correlated to understand the improved IGC resistance of LPBF-316L with La(NO3)3·6H2O additive.}, number={6}, journal={CORROSION}, author={Vukkum, Venkata Bhuvaneswari and Delvecchio, Evan and Christudasjustus, Jijo and Storck, Steven and Gupta, Rajeev Kumar}, year={2023}, month={Jun}, pages={624–636} } @article{o'brien_christudasjustus_delvecchio_birbilis_gupta_2023, title={Microstructure and corrosion of CrFeMnV multi-principal element alloy}, volume={222}, ISSN={["1879-0496"]}, DOI={10.1016/j.corsci.2023.111403}, abstractNote={A multi-principal element alloy consisting of equiatomic concentrations of Cr, Fe, Mn, and V was produced by arc melting. The combination of X-ray diffraction, scanning electron microscopy and energy-dispersive X-ray spectroscopy indicated that the CrFeMnV MPEA was comprised of a BCC matrix with a dispersion of a secondary phase. Cyclic potentiodynamic polarization tests in 0.6 M NaCl revealed high corrosion resistance – superior to that of stainless steel 304L, as evident from high breakdown and repassivation potentials. X-ray photoelectron spectroscopy and time-of-flight secondary ion mass spectrometry provided insight into the formed multi-layer surface film after constant immersion and potentiostatic conditioning.}, journal={CORROSION SCIENCE}, author={O'Brien, S. P. and Christudasjustus, J. and Delvecchio, E. and Birbilis, N. and Gupta, R. K.}, year={2023}, month={Sep} } @article{christudasjustus_witharamage_vukkum_walunj_borkar_gupta_2023, title={Surface Film Formation on Al-V Alloys with Far-From-Equilibrium Microstructure}, volume={170}, ISSN={["1945-7111"]}, url={https://doi.org/10.1149/1945-7111/acc7ce}, DOI={10.1149/1945-7111/acc7ce}, abstractNote={Nanocrystalline supersaturated Al-V alloys produced by high-energy ball milling have been reported to exhibit enhanced corrosion resistance and mechanical properties compared to commercial Al alloys. Corrosion of passive alloys such as Al-V alloy relies on the characteristics of the surface film, which is studied using scanning/transmission electron microscopy and time-of-flight secondary ion mass spectrometry. The effect of microstructure and composition on the surface film has been investigated after different immersion periods (30 min, 2 h, and 1 day) in 0.1 M NaCl. The surface film was complex and composed of oxidized Al and V. The heterogeneous surface film was observed due to the presence of secondary phases and initiation of localized corrosion. The void formation was observed beneath the surface film that would potentially cause pitting corrosion. The generation of nano-sized voids was dependent on grain orientation. Compared to pure Al, the chloride penetration is suppressed in Al-V alloys. The effect of composition and microstructure on surface film formation and attendant corrosion behavior is discussed herein.}, number={3}, journal={JOURNAL OF THE ELECTROCHEMICAL SOCIETY}, author={Christudasjustus, J. and Witharamage, C. S. and Vukkum, V. B. and Walunj, G. and Borkar, T. and Gupta, R. K.}, year={2023}, month={Mar} } @article{witharamage_darwish_christudasjustus_soltis_gupta_2023, title={Time-Dependent Corrosion Behavior of Aluminum Using Advanced Electrochemical and Characterization Techniques}, volume={170}, ISSN={["1945-7111"]}, url={https://doi.org/10.1149/1945-7111/acfb40}, DOI={10.1149/1945-7111/acfb40}, abstractNote={The time-dependent corrosion behavior of pure aluminum (Al) in a chloride-containing environment was investigated using various electrochemical and characterization techniques for up to 336 h. Transmission electron microscopic and secondary ion mass spectroscopic analysis revealed the continuous dissolution of the surface film over the immersion time. In the meantime, the increasing passive oxide thickness resulted in the surface film resistance enhancement over the immersion time, as indicated by the electrochemical impedance spectroscopic analysis. The electrochemical noise measurements showed an increase in the corrosion kinetics with immersion time until 60 h because of the accelerated localized corrosion in the early stage of immersion. However, an inhibition in corrosion kinetics occurred after longer immersion times due to corrosion product deposition inside the pit.}, number={9}, journal={JOURNAL OF THE ELECTROCHEMICAL SOCIETY}, author={Witharamage, C. S. and Darwish, A. A. and Christudasjustus, J. and Soltis, J. and Gupta, R. K.}, year={2023}, month={Sep} } @article{christudasjustus_larimian_esquivel_gupta_darwish_borkar_gupta_2022, title={Aluminum alloys with high elastic modulus}, volume={320}, ISSN={["1873-4979"]}, DOI={10.1016/j.matlet.2022.132292}, abstractNote={Binary Al-5M alloys, containing 5 at.% alloying element (M: Cr, Si, Nb, Mo, and V), have been produced by high-energy ball milling and subsequent spark plasma sintering. X-ray diffraction analysis indicated the solid solubility of the alloying elements to be several orders of magnitude higher than that predicted by the phase diagram. The elastic modulus and hardness of Al-5M alloys, analyzed using nanoindentation, were significantly higher than the commercial Al alloys. High elastic modulus was attributed to the decrease in lattice parameters as a result of the extended solid solubility of the alloying elements.}, journal={MATERIALS LETTERS}, author={Christudasjustus, J. and Larimian, T. and Esquivel, J. and Gupta, S. and Darwish, A. A. and Borkar, T. and Gupta, R. K.}, year={2022}, month={Aug} } @article{ozdemir_witharamage_christudasjustus_darwish_okuyucu_gupta_2022, title={Corrosion behavior of a bulk nanocrystalline Al-Fe alloy}, volume={209}, ISSN={["1879-0496"]}, DOI={10.1016/j.corsci.2022.110727}, abstractNote={Nanocrystalline Al-Fe alloy, with uniform microstructure and high solid solubility of Fe, has been produced by high-energy ball milling. Cyclic potentiodynamic polarization tests revealed high pitting potential. Hardness and corrosion resistance of the Al-Fe alloy were higher than any commercial Al alloy. High hardness and corrosion resistance were attributed to the nanocrystalline structure and formation of solid solution. X-ray photoelectron spectroscopy, secondary ion mass spectrometry, and scanning transmission electron microscopy indicated the incorporation of Fe to the surface film and Fe enrichment at the alloy/surface film interface, which were attributed to the enhanced corrosion performance.}, journal={CORROSION SCIENCE}, author={Ozdemir, F. and Witharamage, C. S. and Christudasjustus, J. and Darwish, A. A. and Okuyucu, H. and Gupta, R. K.}, year={2022}, month={Dec} } @article{witharamage_christudasjustus_smith_gao_gupta_2022, title={Corrosion behavior of an in situ consolidated nanocrystalline Al-V alloy}, volume={6}, ISSN={["2397-2106"]}, url={https://doi.org/10.1038/s41529-022-00225-5}, DOI={10.1038/s41529-022-00225-5}, abstractNote={Abstract}, number={1}, journal={NPJ MATERIALS DEGRADATION}, author={Witharamage, C. S. and Christudasjustus, J. and Smith, J. and Gao, W. and Gupta, R. K.}, year={2022}, month={Feb} } @article{vukkum_christudasjustus_darwish_storck_gupta_2022, title={Enhanced corrosion resistance of additively manufactured stainless steel by modification of feedstock}, volume={6}, ISSN={["2397-2106"]}, url={https://doi.org/10.1038/s41529-021-00215-z}, DOI={10.1038/s41529-021-00215-z}, abstractNote={Abstract}, number={1}, journal={NPJ MATERIALS DEGRADATION}, publisher={Springer Science and Business Media LLC}, author={Vukkum, V. B. and Christudasjustus, J. and Darwish, A. A. and Storck, S. M. and Gupta, R. K.}, year={2022}, month={Jan} } @article{ozdemir_christudasjustus_vukkum_okuyucu_gupta_2022, title={Need of an Inert Atmosphere for High-Energy Ball Milling of Al Alloys}, volume={9}, ISSN={["1544-1024"]}, url={https://doi.org/10.1007/s11665-022-07309-y}, DOI={10.1007/s11665-022-07309-y}, journal={JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE}, author={Ozdemir, F. and Christudasjustus, J. and Vukkum, V. B. and Okuyucu, H. and Gupta, R. K.}, year={2022}, month={Sep} } @article{christudasjustus_witharamage_walunj_borkar_gupta_2022, title={The influence of spark plasma sintering temperatures on the microstructure, hardness, and elastic modulus of the nanocrystalline Al-xV alloys produced by high-energy ball milling}, volume={122}, ISSN={["1005-0302"]}, url={https://doi.org/10.1016/j.jmst.2022.02.008}, DOI={10.1016/j.jmst.2022.02.008}, abstractNote={• Synthesis of Al-V alloys from high-energy ball milling and spark plasma sintering. • Al-V alloys with far-from-equilibrium microstructure: V solubility 6 orders of magnitude higher than equilibrium value. • Elastic modulus of Al-V alloys is much higher than that of any commercial Al alloy. • Effect of spark plasma sintering temperature on the microstructure, hardness and elastic modulus of Al-V alloys. Al- x V alloys ( x = 2 at.%, 5 at.%, 10 at.%) with nanocrystalline structure and high solid solubility of V were produced in powder form by high-energy ball milling (HEBM). The alloy powders were consolidated by spark plasma sintering (SPS) employing a wide range of temperatures ranging from 200 to 400 °C. The microstructure and solid solubility of V in Al were investigated using X-ray diffraction analysis, scanning electron microscope and transmission electron microscope. The microstructure was influenced by the SPS temperature and V content of the alloy. The alloys exhibited high solid solubility of V―six orders of magnitude higher than that in equilibrium state and grain size < 50 nm at all the SPS temperatures. The formation of Al 3 V intermetallic was detected at 400 °C. Formation of a V-lean phase and bimodal grain size was observed during SPS, which increased with the increase in SPS temperature. The hardness and elastic modulus, measured using nanoindentation, were significantly higher than commercial alloys. For example, Al-V alloy produced by SPS at 200 °C exhibited a hardness of 5.21 GPa along with elastic modulus of 96.21 GPa. The evolution of the microstructure and hardness with SPS temperatures has been discussed.}, journal={JOURNAL OF MATERIALS SCIENCE & TECHNOLOGY}, publisher={Elsevier BV}, author={Christudasjustus, J. and Witharamage, C. S. and Walunj, Ganesh and Borkar, T. and Gupta, R. K.}, year={2022}, month={Sep}, pages={68–76} } @article{o'brien_christudasjustus_esteves_vijayan_jinschek_birbilis_gupta_2021, title={A low-cost, low-density, and corrosion resistant AlFeMnSi compositionally complex alloy}, volume={5}, ISSN={["2397-2106"]}, url={https://doi.org/10.1038/s41529-021-00158-5}, DOI={10.1038/s41529-021-00158-5}, abstractNote={Abstract}, number={1}, journal={NPJ MATERIALS DEGRADATION}, publisher={Springer Science and Business Media LLC}, author={O'Brien, S. P. and Christudasjustus, J. and Esteves, L. and Vijayan, S. and Jinschek, J. R. and Birbilis, N. and Gupta, R. K.}, year={2021}, month={Mar} } @article{esteves_witharamage_christudasjustus_walunj_o'brien_ryu_borkar_akans_gupta_2021, title={Corrosion behavior of AA5083 produced by high-energy ball milling}, volume={857}, ISSN={["1873-4669"]}, url={http://www.scopus.com/inward/record.url?eid=2-s2.0-85098468414&partnerID=MN8TOARS}, DOI={10.1016/j.jallcom.2020.158268}, abstractNote={The corrosion, microstructure, and hardness of nanocrystalline AA5083 were compared to that of conventional AA5083-H116 and consolidated gas atomized powder. The nanocrystalline AA5083 was produced by consolidating high-energy ball milled gas atomized powder with two methods: cold compaction and spark plasma sintering. Electrochemical impedance spectroscopy, cyclic potentiodynamic polarization, Mott-Schottky analysis, and immersion tests followed by surface analysis were used to evaluate the corrosion behavior in 0.6 M NaCl solution. Pitting corrosion resistance of the nanocrystalline AA5083 was superior to that of commercial AA5083-H116. The improved corrosion resistance was primarily attributed to the homogenous microstructure and significant grain refinement below 100 nm.}, journal={JOURNAL OF ALLOYS AND COMPOUNDS}, publisher={Elsevier BV}, author={Esteves, L. and Witharamage, C. S. and Christudasjustus, J. and Walunj, G. and O'Brien, S. P. and Ryu, S. and Borkar, T. and Akans, R. E. and Gupta, R. K.}, year={2021}, month={Mar} } @article{esteves_christudasjustus_o'brien_witharamage_darwish_walunj_stack_borkar_akans_gupta_2021, title={Effect of V content on corrosion behavior of high-energy ball milled AA5083}, volume={186}, ISSN={["1879-0496"]}, url={https://doi.org/10.1016/j.corsci.2021.109465}, DOI={10.1016/j.corsci.2021.109465}, abstractNote={AA5083 alloys with V additions were produced in the powder form by high-energy ball milling and consolidation by spark plasma sintering and cold compaction. X-ray diffraction and energy dispersive X-ray spectroscopy analysis indicated the formation of supersaturated solid solution and grain refinement below 100 nm. Corrosion behavior was investigated using electrochemical impedance spectroscopy, cyclic potentiodynamic polarization, and immersion corrosion tests followed by surface analysis. The composition of the passive film was obtained via X-ray photoelectron spectroscopy. The corrosion resistance of the AA5083 was significantly improved due to the addition of V and high-energy ball milling.}, journal={CORROSION SCIENCE}, publisher={Elsevier BV}, author={Esteves, L. and Christudasjustus, J. and O'Brien, S. P. and Witharamage, C. S. and Darwish, A. A. and Walunj, G. and Stack, P. and Borkar, T. and Akans, R. E. and Gupta, R. K.}, year={2021}, month={Jul} } @article{witharamage_christudasjustus_gupta_2021, title={The Effect of Milling Time and Speed on Solid Solubility, Grain Size, and Hardness of Al-V Alloys}, volume={30}, ISSN={["1544-1024"]}, url={http://dx.doi.org/10.1007/s11665-021-05663-x}, DOI={10.1007/s11665-021-05663-x}, number={4}, journal={JOURNAL OF MATERIALS ENGINEERING AND PERFORMANCE}, publisher={Springer Science and Business Media LLC}, author={Witharamage, C. S. and Christudasjustus, J. and Gupta, R. K.}, year={2021}, month={Apr}, pages={3144–3158} } @inbook{walunj_bearden_patil_larimian_christudasjustus_gupta_borkar_2021, place={Cham, Switzerland}, title={The Effect of Titanium Carbide and Spark Plasma Sintering Processing on Nickel–Titanium Carbide Composites}, ISBN={9783030652494}, url={http://www.scopus.com/inward/record.url?eid=2-s2.0-85102048699&partnerID=MN8TOARS}, DOI={10.1007/978-3-030-65249-4_4}, booktitle={Metal-Matrix Composites: Advances in Analysis, Measurement, and Observations}, publisher={Springer Nature}, author={Walunj, G. and Bearden, A. and Patil, A. and Larimian, T. and Christudasjustus, J. and Gupta, R.K. and Borkar, T.}, editor={Srivatsan, T.S. and Harrigan, W.C., Jr/ and Hunyadi Murph, S.Editors}, year={2021}, pages={65–73} } @article{larimian_chaudhary_christudasjustus_ramanujan_gupta_borkar_2020, title={Bulk-nano spark plasma sintered Fe-Si-B-Cu-Nb based magnetic alloys}, volume={124}, ISSN={0966-9795}, url={http://dx.doi.org/10.1016/j.intermet.2020.106869}, DOI={10.1016/j.intermet.2020.106869}, abstractNote={Iron-based soft magnetic alloys (FeSiB, FeSiBNb, FeSiBCu, and FeSiBNbCu (Finemet)) have been fabricated via mechanical alloying followed by spark plasma sintering (SPS) process. FeSiB alloy powder was obtained by high energy ball milling of an elemental blend Fe, Si, and B powders. The effect of milling time on crystallite size and phase transformation was studied. Additionally, FeSiBCu, FeSiBNb, and FeSiBCuNb alloy powders were milled to study the effect of Cu and Nb on phase transformation, mechanical, and magnetic behavior. The mechanically alloyed powders were sintered via SPS process to achieve full densification. The microhardness and magnetic permeability of sintered FeSiB alloys were found to be increased monotonically with milling time primarily due to the smaller crystallite size and more uniform microstructure. Interestingly, the alloying of Cu or (and) Nb to FeSiB resulted in higher saturation magnetization and lower coercivity mainly due to large volume fraction of α-Fe3Si nanocrystals. Overall, these alloys exhibit reasonably good soft magnetic behavior along with excellent microhardness. Mechanical alloying followed by spark plasma sintering opens up a new avenue of processing amorphous-nanocrystalline alloys into bulk shape with good mechanical and magnetic properties.}, journal={Intermetallics}, publisher={Elsevier BV}, author={Larimian, T. and Chaudhary, V. and Christudasjustus, J. and Ramanujan, R.V. and Gupta, R. and Borkar, T.}, year={2020}, month={Sep}, pages={106869} } @article{walunj_bearden_patil_larimian_christudasjustus_gupta_borkar_2020, title={Mechanical and Tribological Behavior of Mechanically Alloyed Ni-TiC Composites Processed via Spark Plasma Sintering}, volume={13}, ISSN={["1996-1944"]}, url={https://doi.org/10.3390/ma13225306}, DOI={10.3390/ma13225306}, abstractNote={Titanium carbide (TiC) reinforced nickel (Ni) matrix composites were processed via mechanical alloying (MA) followed by spark plasma sintering (SPS) process. Mechanical alloying has gained special attention as a powerful non-equilibrium process for fabricating amorphous and nanocrystalline materials, whereas spark plasma sintering (SPS) is a unique technique for processing dense and near net shape bulk alloys with homogenous microstructure. TiC reinforcement varied from 5 to 50 wt.% into nickel matrix to investigate its effect on the microstructure and mechanical behavior of Ni-TiC composites. All Ni-TiC composites powder was mechanically alloyed using planetary high energy ball mill with 400 rpm and ball to powder ratio (BPR) 15:1 for 24 h. Bulk Ni-TiC composites were then sintered via SPS process at 50 MPa pressure and 900–1200 °C temperature. All Ni-TiC composites exhibited higher microhardness and compressive strength than pure nickel due to the presence of homogeneously distributed TiC particles within the nickel matrix, matrix grain refinement, and excellent interfacial bonding between nickel and TiC reinforcement. There is an increase in Ni-TiC composites microhardness with an increase in TiC reinforcement from 5 to 50 wt.%, and it reaches the maximum value of 900 HV for Ni-50TiC composites.}, number={22}, journal={MATERIALS}, publisher={MDPI AG}, author={Walunj, Ganesh and Bearden, Anthony and Patil, Amit and Larimian, Taban and Christudasjustus, Jijo and Gupta, Rajeev Kumar and Borkar, Tushar}, year={2020}, month={Nov} } @article{khan_patil_christudasjustus_borkar_gupta_2020, title={Spark plasma sintering of a high-energy ball milled Mg-10 wt% Al alloy}, volume={8}, url={https://doi.org/10.1016/j.jma.2020.02.006}, DOI={10.1016/j.jma.2020.02.006}, abstractNote={The influence of spark plasma sintering (SPS) temperature on microstructure, hardness and corrosion behavior of a high-energy ball milled Mg-10 wt% Al alloy was investigated in this work. The holding time and sintering pressure for SPS were kept constant while varying the sintering temperature from 200 to 350 °C. The grain size and microstructure were studied using X-ray diffraction analysis, scanning electron microscopy, energy dispersive X-ray spectroscopy, and Archimedes’ based density measurement. Corrosion behavior was investigated using potentiodynamic polarization tests. The nanocrystalline regime (grain size < 100 nm) was maintained even after SPS up to 350 °C. The density of the alloy increased with increasing the SPS temperature. Vickers’ hardness and corrosion performance improved up to 300 °C followed by a decrease after SPS at 350 °C. Possible reasons for densification, strengthening, and corrosion behavior have been discussed in the light of reduced porosity and microstructural changes.}, number={2}, journal={Journal of Magnesium and Alloys}, publisher={Elsevier BV}, author={Khan, M.U.F. and Patil, A. and Christudasjustus, J. and Borkar, T. and Gupta, R.K.}, year={2020}, month={Jun}, pages={319–328} }