@article{escobar_silverstein_ishrak_li_soulami_li_yu_mathaudhu_ortiz_koch_et al._2023, title={Microstructural evolution in shear-punch tests: A comparative study of pure Cu and Cu-Cr alloy}, volume={886}, ISSN={["1873-4936"]}, url={https://doi.org/10.1016/j.msea.2023.145715}, DOI={10.1016/j.msea.2023.145715}, abstractNote={Understanding the mechanisms behind microstructural evolution during shear deformation has been a long-standing area of interest. However, establishing a connection between microstructure, mechanical properties, and the extent of shear deformation is challenging and requires refined experimental approaches. Shear-punch testing (SPT) provides a controlled method to introduce shear into small volumes of material that later can be subjected to detailed microstructural characterization. In this study, we utilize an SPT device to induce shear deformation to pure copper (Cu) and a binary copper-chromium (Cu-Cr) alloy. Electron backscatter diffraction and transmission electron microscopy were used to study the mechanisms of plastic deformation after SPT. Our results indicate that shear deformation of pure Cu produces a dense network of intercepting microshear bands upon sustained deformation. Twin boundaries in annealed Cu undergo transformation into high-angle grain boundaries due to simultaneous deviation from the axis-angle pair condition of 60° misorientation on [111] direction. The presence of 50 vol% Cr particles in the soft Cu matrix altered the shear deformation mechanism. Preferential deformation of the Cu matrix in Cu-Cr alloy led to accelerated shear-induced formation of low and high-angle grain boundaries and subsequent grain refinement. Comparatively, insignificant grain refinement occurred in pure Cu samples even at a strain ∼10 times larger (ε = 4.73) than that of the Cu-Cr case (ε = 0.42). This study sheds light on the microstructural evolution of Cu during shear deformation and highlights the significant influence of a hard second phase in modifying the microstructural response mechanisms of a softer matrix.}, journal={MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING}, author={Escobar, Julian and Silverstein, Joshua and Ishrak, Farhan and Li, Lei and Soulami, Ayoub and Li, Shuang and Yu, Anqi and Mathaudhu, Suveen and Ortiz, Angel and Koch, Carl and et al.}, year={2023}, month={Oct} } @article{gu_zhu_mathaudhu_2015, title={A model for < c plus a & rang; dislocation transmission across nano-spaced parallel basal stacking faults in a HCP alloy}, volume={95}, ISSN={["1362-3036"]}, DOI={10.1080/09500839.2015.1008066}, abstractNote={We develop a model for recently observed 〈c + a〉 dislocation transmission across nano-spaced parallel basal stacking faults in hexagonal close-packed (HCP) Mg microcrystalline grains. The model theoretically predicts nanospace-dependent yield strength that is in good agreement with experimental data. Additionally, it theoretically predicts activation volume and strain rate sensitivity.}, number={1}, journal={PHILOSOPHICAL MAGAZINE LETTERS}, author={Gu, Pei and Zhu, Yuntian and Mathaudhu, Suveen N.}, year={2015}, month={Jan}, pages={58–66} } @article{zhou_xu_jian_cheng_ma_guo_mathaudhu_wang_zhu_2014, title={A new metastable precipitate phase in Mg-Gd-Y-Zr alloy}, volume={94}, ISSN={["1478-6443"]}, DOI={10.1080/14786435.2014.913115}, abstractNote={Mg–RE alloys are among the strongest Mg-based alloys due to their unique precipitation structures. A previously unobserved metastable phase (βT) is found to coexist with reported β″ and β′ metastable phases under peak ageing conditions in a Mg–Gd–Y–Zr alloy. The position of the RE elements within the βT phase is identified using atomic-resolution high-angle annular dark field scanning transmission electron microscopy imaging, and the βT phase is shown to have an orthorhombic structure with a stoichiometry of Mg5RE. Based on these observations, a new precipitation sequence is proposed.}, number={21}, journal={PHILOSOPHICAL MAGAZINE}, author={Zhou, H. and Xu, W. Z. and Jian, W. W. and Cheng, G. M. and Ma, X. L. and Guo, W. and Mathaudhu, S. N. and Wang, Q. D. and Zhu, Y. T.}, year={2014}, pages={2403–2409} } @article{piyawit_xu_mathaudhu_freudenberger_rigsbee_zhu_2014, title={Nucleation and growth mechanism of Ag precipitates in a CuAgZr alloy}, volume={610}, ISSN={["1873-4936"]}, DOI={10.1016/j.msea.2014.05.023}, abstractNote={CuAgZr alloy is a variant of the CuAg alloy that is developed for high strength and high conductivity applications. Its strengthening is accomplished mainly by the precipitation of Ag precipitates, which tend to align on {111} planes in the Cu matrix. This alignment has been reported to be caused by stacking faults on {111} planes. Contrary to these reports, this research presents evidence for Ag precipitates formation on {111} planes due to the minimization of elastic energy. The Ag precipitates were formed by clustering of Ag atoms while maintaining the fcc crystal structure of the matrix. They have faceted {111} interfaces with the matrix. The thickening of precipitates appears to be by the ledge growth mechanism, which is resulted in by misfit dislocation networks on the interface.}, journal={MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING}, author={Piyawit, W. and Xu, W. Z. and Mathaudhu, S. N. and Freudenberger, J. and Rigsbee, J. M. and Zhu, Y. T.}, year={2014}, month={Jul}, pages={85–90} } @article{jian_cheng_xu_koch_wang_zhu_mathaudhu_2013, title={Physics and model of strengthening by parallel stacking faults}, volume={103}, ISSN={0003-6951 1077-3118}, url={http://dx.doi.org/10.1063/1.4822323}, DOI={10.1063/1.4822323}, abstractNote={We have recently reported that parallel stacking faults (SFs) can tremendously increase the strength of a magnesium alloy. The strengthening is found to increase linearly with the reciprocal of the mean SF spacing, d. In this study we analyze dislocation interactions with SFs, and then propose a physics-based model to explain the observed relationship between yield strength and SFs spacing. Similar to the empirical Hall-Petch relationship for grain size, it is expected that this strengthening mechanism will hold true for a variety of materials engineered with parallel spaced stacking faults over a wide range of fault spacing.}, number={13}, journal={Applied Physics Letters}, publisher={AIP Publishing}, author={Jian, W. W. and Cheng, G. M. and Xu, W. Z. and Koch, C. C. and Wang, Q. D. and Zhu, Y. T. and Mathaudhu, S. N.}, year={2013}, month={Sep}, pages={133108} } @book{mathaudhu_sillekens_neelameggham_hort_2012, title={Magnesium technology 2012: proceedings of a symposium sponsored by the Magnesium Committee of the Light Metals Division of the Minerals, Metals & Materials Society (TMS), held during TMS 2012 Annual Meeting & Exhibition, Orlando Florida, USA, March11-15}, publisher={Warrendale, Pennsylvania: The Minerals, Metals and Materials Society}, year={2012} }